英语翻译E.General Method for Esterification.EDC HCl (4 mmo
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英语翻译
E.General Method for Esterification.EDC HCl (4 mmol ×
free OH) was added in one solid portion to a solution of DMAP
(0.6 equiv in SM) PEG-COOH (4 mmol × free OH),and either
Lam-D (15)or 18 (1 mmol) in dry CH2Cl2 (45 mL).The
resulting solution was stirred at r.t.for 3 h.The reaction mixture
was diluted with CH2Cl2 and washed with sat.aq.NaHCO3 and
brine.The organic phase was dried over anhydrous MgSO4,and
the solvent was removed under vacuum.The residue was
directly purified on silica gel to provide compounds 8,9,19a f
(40% quant.yield).
E.General Method for Esterification.EDC HCl (4 mmol ×
free OH) was added in one solid portion to a solution of DMAP
(0.6 equiv in SM) PEG-COOH (4 mmol × free OH),and either
Lam-D (15)or 18 (1 mmol) in dry CH2Cl2 (45 mL).The
resulting solution was stirred at r.t.for 3 h.The reaction mixture
was diluted with CH2Cl2 and washed with sat.aq.NaHCO3 and
brine.The organic phase was dried over anhydrous MgSO4,and
the solvent was removed under vacuum.The residue was
directly purified on silica gel to provide compounds 8,9,19a f
(40% quant.yield).
![英语翻译E.General Method for Esterification.EDC HCl (4 mmo](/uploads/image/z/19066317-69-7.jpg?t=%E8%8B%B1%E8%AF%AD%E7%BF%BB%E8%AF%91E.General+Method+for+Esteri%26%2364257%3Bcation.EDC+HCl+%284+mmo)
一般方法,即酯化反应.(四mmol×盐酸EDC)
免费的哦)中增加了一份对解决这一问题的深度贴图
(在SM)为PEG-COOH(4 mmol×自由哦),要么
Lam-D(15)或18岁(1)在干燥mmol以(45毫升).这个
在解决方案都是造成3小时r.t..反应
被稀释,用sat.以类似.NaHCO3和
盐水.有机相是在无水MgSO4、干燥
在真空环境下的溶剂被移除.剩下的是
直接净化硅胶为化合物8、9、种在f
(40% quant.产量).
免费的哦)中增加了一份对解决这一问题的深度贴图
(在SM)为PEG-COOH(4 mmol×自由哦),要么
Lam-D(15)或18岁(1)在干燥mmol以(45毫升).这个
在解决方案都是造成3小时r.t..反应
被稀释,用sat.以类似.NaHCO3和
盐水.有机相是在无水MgSO4、干燥
在真空环境下的溶剂被移除.剩下的是
直接净化硅胶为化合物8、9、种在f
(40% quant.产量).
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